Synthesis and solubility of a new polyimide dianhydride monomer

Expand
  • Department of Biochemistry,Nanchang University College of Science and Technology,Nanchang 330029

Received date: 2019-04-04

  Revised date: 2020-04-06

  Online published: 2020-10-23

Abstract

Furan and maleic anhydride as solvent,a new target product of dianhydride monomer was synthesized by D-A addition,nucleophile substitution and decyclization,etc.The structures of intermediates and dianhydride monomer were characterized by 1H-NMR spectra,and indicated that the synthesis was successfully performed.This target product can dissolved in common solvent on the basis of the solubility test which was very helpful for the subsequent synthesis of polyimide.

Cite this article

Xiong Bing, Tang Mingbei, Fan Decai, Feng Simao . Synthesis and solubility of a new polyimide dianhydride monomer[J]. New Chemical Materials, 2020 , 48(8) : 174 -176 . DOI: 10.19817/j.cnki.issn 1006-3536.2020.08.038

References

[1] 丁孟贤.聚酰亚胺—化学、结构与性能的关系及材料[M].北京:科学出版社,2006.
[2] 周纪,金海兰.聚酰亚胺复合材料的应用研究进展[J].纸和造纸,2017,36(2):14-17.
[3] 杨家义,杨博峰,郑国运,等.热固性聚酰亚胺树脂成型工艺研究进展[J].功能材料,2018,49(2):2054-2059.
[4] 何志富,黄凯,高蔓彤,等.可溶性聚酰亚胺膜的制备及其纳滤分离特性研究[J].膜科学与技术,2018,38(4):70-74.
[5] 鲁云华,胡知之,王永飞,等.可溶性浅色透明聚酰亚胺的研究进展[J].材料导报,2011,25(3):64-68.
[6] Masatoshi,Hasegawa,Daiki Hirano,et al.Solution-processable colorless polyimides derived from hydrogenated pyromellitic dianhydride with controlled steric structure[J].J Polym Sci A Polym Chem,2012,51(3):575-592.
[7] Ma Tao,Zhang Shujiang,Li Yanfeng,et al.Synthesis and characterization of soluble polyimides based on a new fluorinated diamine:4-phenyl-2,6-bis[3-(4′-amino-2′-trifluoromethyl-phenoxy)phenyl]pyridine[J].Journal of Fluorine Chemistry,2010,131(6):724-730.
[8] 高冠群,董亮,刘向阳,等.杂环二胺改性PMDA/ODA型聚酰亚胺纤维性能的研究[C].2007年全国高分子学术论文报告会论文摘要集(下册).2007.
[9] 熊兵,刘峰,张旭华.一种新型耐高温聚酰亚胺低聚物的研究[J].化工新型材料,2009,37(1):36-37.
Options
Outlines

/