GO/WO3复合材料的制备及对三乙胺气敏性能研究

张玲, 轩岩岩, 张慧敏, 吕露, 袁颖楠, 常薇, 刘斌*

化工新型材料 ›› 2025, Vol. 53 ›› Issue (2) : 159 -162.

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化工新型材料 ›› 2025, Vol. 53 ›› Issue (2) : 159-162. DOI: 10.19817/j.cnki.issn1006-3536.2025.02.009
科学研究

GO/WO3复合材料的制备及对三乙胺气敏性能研究

    张玲, 轩岩岩, 张慧敏, 吕露, 袁颖楠, 常薇, 刘斌*
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Preparation of GO/WO3 composite and its gas sensitivity to triethylamine

  • Zhang Ling, Xuan Yanyan, Zhang Huimin, Lv Lu, Yuan Yingnan, Chang Wei, Liu Bin
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摘要

通过超声复合制备了氧化石墨烯GO含量不同(质量分数分别为2.5%,5%,10%)的氧化石墨烯/氧化钨(GO/WO3)复合材料,通过X射线衍射仪、场发射扫描电子显微镜和傅里叶变换红外光谱仪、气敏元件测试仪对复合材料的结构、形貌和气敏性能进行了表征和测试。结果表明:制备的GO/WO3复合材料对三乙胺具有良好的选择性和稳定性;最佳工作温度为190℃时,对100ppm三乙胺气体的灵敏度达到了12.1;响应时间和恢复时间分别为21s和29s。

Abstract

GO/WO3 nanocomposites with different doping ratios (mass fractions of 2.5%,5%,10%) were prepared by ultrasound compounding method.The structure,morphology and gas sensitivity of the composite were characterized and tested using X-ray diffraction (XRD),scanning electron microscopy (SEM),and infrared spectroscopy (FT-IR).The results showed that the prepared gas sensing element exhibited excellent selectivity and stability for triethylamine.At an optimal operating temperature of 190℃,the sensitivity to 100 ppm triethylamine gas reached 12.1.In addition,the response time and recovery time were 21 s and 29 s,respectively.

关键词

氧化钨 / 氧化石墨烯 / 三乙胺 / 复合材料 / 气敏性能

Key words

WO3 / graphene oxide / triethylamine / composite / gas sensitivity

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GO/WO3复合材料的制备及对三乙胺气敏性能研究[J]. 化工新型材料, 2025, 53(2): 159-162 DOI:10.19817/j.cnki.issn1006-3536.2025.02.009

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基金资助

陕西省科技计划项目(2021KW-12);西安工程大学省级大学生创新训练计划项目(S202210709125)

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