预制体浸渗法苎麻纤维织物遗态结构Al2O3-Cu复合材料的制备及其性能研究

李笑然1, 王俊勃1*, 胡新煜1, 姜凤阳2, 王蒙1

化工新型材料 ›› 2019, Vol. 47 ›› Issue (5) : 100 -103.

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化工新型材料 ›› 2019, Vol. 47 ›› Issue (5) : 100-103.
新材料与新技术

预制体浸渗法苎麻纤维织物遗态结构Al2O3-Cu复合材料的制备及其性能研究

    李笑然1, 王俊勃1*, 胡新煜1, 姜凤阳2, 王蒙1
作者信息 +

Preparation and property of ramie fiber fabric legacy Al2O3-Cu with preform infiltration

  • Li Xiaoran1, Wang Junbo1, Hu Xinyu1, Jiang Fengyang2, Wang Meng1
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摘要

采用预制体浸渗法制备苎麻纤维织物遗态结构Al2O3-Cu复合材料,利用X射线衍射仪、扫描电子显微镜和能谱分析仪研究复合材料的物相组成及微观形貌,并进行拉伸试验研究。结果表明:Al2O3陶瓷预制体完整地保留了苎麻纤维织物遗态结构,经氧化浸渍形成了由CuO和偏铝酸亚铜(CuAlO2)包覆Al2O3为组织特征的柱状铆接结构。经1020℃还原烧结,Cu相与本体Al2O3相和析出CuAlO2相共融互渗,形成了由Cu保护层覆盖、以交叉片状组织(Cu+Al2O3+CuAlO2)为内衬的Al2O3-Cu复合材料,其拉伸强度为10.73MPa。

Abstract

The phase composition and microstructure of ramie fiber fabric legacy structure Al2O3-Cu composite materials with preform infiltration method were investigated by means of XRD,SEM and EDS.Tensile tests were conducted.The results showed that Al2O3 preform retained the complete ramie fiber fabric heritage structure.Oxidation impregnation samples formed a columnar riveted structure which tissue feature was CuO and CuAlO2 coated Al2O3.After reduction and sintering at 1020℃,the Cu phase co-melted with the bulk Al2O3 phase and the precipitated CuAlO2 phase.The outer surface of Al2O3-Cu was covered by Cu protective layer and the inner core was cross-sectioned (Cu+Al2O3+CuAlO2).And its tensile strength was 10.73MPa.

关键词

预制体浸渗法 / 苎麻纤维织物 / 遗态结构 / Al2O3-Cu

Key words

preform infiltration method / ramie fiber fabric / heritage structure / Al2O3-Cu

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预制体浸渗法苎麻纤维织物遗态结构Al2O3-Cu复合材料的制备及其性能研究[J]. 化工新型材料, 2019, 47(5): 100-103 DOI:

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基金资助

国家自然科学基金(21603169);陕西省科技攻关项目(2016-GY014);西安工程大学研究生创新基金项目(CX201704)

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