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化工新型材料  2018, Vol. 46 Issue (7): 81-84    
  新材料与新技术 本期目录 | 过刊浏览 | 高级检索 |
水热法制备氧化石墨烯负载TiO2的研究
林春玲1, 焦小妮2, 周玲1, 常木蓝1, 刘明杰1
1.西安石油大学化学化工学院,西安710065;
2.长庆油田分公司第四采气厂,西安710021
Study on hydrothermal synthesis of graphene loaded titanium dioxide (GO/TiO2)
Lin Chunling1, Jiao Xiaoni2, Zhou Ling1, Chang Mulan1, Liu Mingjie1
1.School of Chemistry and Chemical Engineering,Xi’an University of Petroleum,Xi’an 710065;
2.Fourth Gas Production Plant,Changqing Oilfield Branch,Xi’an 710021;
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摘要 通过水热反应采用氧化石墨烯和TiCl3溶液制备TiO2/石墨烯复合材料。实验研究了反应时间、反应温度对产率的影响。采用红外光谱、X射线衍射、拉曼光谱、紫外-可见分光光度计、扫描电子显微镜、热重分析法等手段对TiO2/氧化石墨烯复合材料的微观结构进行分析。结果表明:利用氧化石墨烯的氧化性与三氯化钛溶液制备出氧化石墨烯负载TiO2的复合材料,复合材料具有良好的热稳定性和优良的光学性能。
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林春玲
焦小妮
周玲
常木蓝
刘明杰
关键词:  氧化石墨烯  负载  水热合成法  TiO2    
Abstract: Composite (GO/TiO2) was prepared with graphene oxide and TiCl3 solution by hydrothermal reaction.The time and temperature of reaction were determined through yield.The sample was analyzed by FT-IR spectroscopy,XRD,Ramans,UV-Vis,SEM and TGA.The results showed that it was prepared by oxidation of graphene oxide and titanium trichloride solution system,This (GO/TiO2) composite materials had good thermal stability.
Key words:  graphene oxide    loading    hydrothermal synthesis    TiO2
收稿日期:  2017-03-06                出版日期:  2018-07-20      发布日期:  2018-08-07      期的出版日期:  2018-07-20
基金资助: 国家自然科学基金(51402132);陕西省教育厅专项科研计划项目(16JK1612);国家级大学生科研训练计划项目(201610705027)
作者简介:  林春玲(1973-),女,硕士,高级工程师,主要研究方向为水处理与高分子材料应用。
引用本文:    
林春玲, 焦小妮, 周玲, 常木蓝, 刘明杰. 水热法制备氧化石墨烯负载TiO2的研究[J]. 化工新型材料, 2018, 46(7): 81-84.
Lin Chunling, Jiao Xiaoni, Zhou Ling, Chang Mulan, Liu Mingjie. Study on hydrothermal synthesis of graphene loaded titanium dioxide (GO/TiO2). New Chemical Materials, 2018, 46(7): 81-84.
链接本文:  
http://www.hgxx.org/CN/  或          http://www.hgxx.org/CN/Y2018/V46/I7/81
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